12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

Base Information

Chemical Name:12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol
CAS No.:725712-07-2
Molecular Formula:C₅₂H₉₀O₆
Molecular Weight:811.283
Hs Code.:

Synonyms:12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

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Chemical Property of 12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

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Technology Process of 12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

There total 1 articles about 12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 5675-51-4
1,12-dodecandiol

: 91-13-4
α,α'-dibromo-o-xylene

: 725712-05-0
12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecan-1-ol

: 725712-07-2
12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1002/ejoc.200300792

Reference yield: 93.0%

: 725712-07-2
12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

: 725712-19-6
12-(2-{12-[2-(12-oxo-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecanal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In triethylamine;
DOI:10.1002/ejoc.200300792

Reference yield:

: 725712-07-2
12-(2-{12-[2-(12-hydroxy-dodecyloxymethyl)-benzyloxy]-dodecyloxymethyl}-benzyloxy)-dodecan-1-ol

: C₅₈H₉₀O₆

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / oxalyl chloride; DMSO / triethylamine

2: 73 percent / DIBAH / -78 - 20 °C

3: 90 percent / Dess-Martin periodine / CH₂Cl₂ / 20 °C

4: 62 percent / AgNO₃ / acetone

With oxalyl dichloride; diisobutylaluminium hydride; Dess-Martin periodane; silver nitrate; dimethyl sulfoxide; In dichloromethane; triethylamine; acetone; 1: Swern oxidation;
DOI:10.1002/ejoc.200300792