6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien

Base Information

• Chemical Name: 6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien
• CAS No.: 124685-98-9
• Molecular Formula: C₂₉H₄₃NO₂
• Molecular Weight: 437.666

Synonyms:6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien

Chemical Property of 6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien

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Technology Process of 6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien

There total 1 articles about 6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>nona-6,8-dien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,3,4-Tri-tert-butylcyclobutadien-1-carbonsaeure-tert-butylester (83747-03-9) + 3-phenyl-2H-azirine (7654-06-0) → 6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.02,4>nona-6,8-dien (124685-98-9)

Guidance literature:

In pentane; at -78 ℃;

Reference yield: 98.0%

6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.02,4>nona-6,8-dien (124685-98-9) → 1,8,9-Tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.02,4>non-8-en-6-on (124686-05-1)

Guidance literature:

In benzene; at 80 ℃; for 168h;

Reference yield:

6-tert-Butoxy-1,8,9-tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.02,4>nona-6,8-dien (124685-98-9) → 2-(Benzoylmethyl)-1,5,6-tri-tert-butyl-2-azabicyclo<2.2.0>hex-5-en-3-on (124686-10-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / benzene / 168 h / 80 °C

2: 38 percent / CHCl₃ / 1.75 h / 10 °C / Irradiation

In chloroform; benzene;

upstream raw materials:

2,3,4-Tri-tert-butylcyclobutadien-1-carbonsaeure-tert-butylester

3-phenyl-2H-azirine

Downstream raw materials:

1,8,9-Tri-tert-butyl-4-phenyl-5-oxa-2-azatricyclo<5.2.0.0^2,4>non-8-en-6-on

2-(Benzoylmethyl)-1,5,6-tri-tert-butyl-2-azabicyclo<2.2.0>hex-5-en-3-on

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