12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

Base Information

• Chemical Name: 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione
• CAS No.: 848086-53-3
• Molecular Formula: C₆₉H₅₉N₃O₉
• Molecular Weight: 1074.24

Synonyms:12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

Chemical Property of 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

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Technology Process of 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

There total 2 articles about 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

3-(6-Benzyloxy-1H-indol-3-yl)-4-[5-benzyloxy-1-((2R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-1H-indol-3-yl]-1-methyl-pyrrole-2,5-dione → 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione (848086-53-3)

Guidance literature:

With palladium dichloride; In N,N-dimethyl-formamide; at 110 ℃; for 1h;

DOI:10.1016/S0040-4020(97)00286-X

Reference yield:

3-(6-Benzyloxy-1H-indol-3-yl)-4-[5-benzyloxy-1-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-1H-indol-3-yl]-1-methyl-pyrrole-2,5-dione (848086-47-5) → 12,13-dihydro-3,10-dibenzyloxy-13-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-5H-indolo[2,3-a]-pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione (848086-53-3)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene;

DOI:10.1016/S0960-894X(99)00595-8

upstream raw materials:

3-(6-Benzyloxy-1H-indol-3-yl)-4-[5-benzyloxy-1-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-1H-indol-3-yl]-1-methyl-pyrrole-2,5-dione

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