Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

Base Information

Chemical Name:Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)
CAS No.:918800-76-7
Molecular Formula:C₁₇H₂₇BrMgO₈
Molecular Weight:463.606
Hs Code.:

Synonyms:Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

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Chemical Property of Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

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Technology Process of Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

There total 2 articles about Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73875-28-2
6-Bromo-2,3-dimethoxy-5-methylhydroquinone bis<2-methoxyethoxymethyl ether>

: 918800-76-7
Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

Guidance literature:: With iodine; magnesium; In tetrahydrofuran; at 40 - 45 ℃; for 2h; Product distribution / selectivity;

Reference yield:

: 73875-28-2
6-Bromo-2,3-dimethoxy-5-methylhydroquinone bis<2-methoxyethoxymethyl ether>

: 7439-95-4
magnesium

: 918800-76-7
Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

Guidance literature:: With iodine; In tetrahydrofuran; at 20 ℃; Product distribution / selectivity;

Reference yield: 70.0%

: 918800-76-7
Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether)

: 1838-94-4
isoprene epoxide

: 918823-43-5
6-(4-hydroxy-3-methyl-2-butenyl)-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl)ether

Guidance literature:: Grignard reagent 6-bromo-2,3-dimethoxy-5-methyl-1,4-hydroquinone bis(2-methoxyethoxymethyl ether); isoprene epoxide; copper(l) chloride; In tetrahydrofuran; at -50 ℃; for 3h;

With ammonium chloride; In tetrahydrofuran; water; Product distribution / selectivity;