Technology Process of C38H69N5O6SSi
There total 1 articles about C38H69N5O6SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / methanol; ethanol / 15.5 h
1.2: 1.5 h
2.1: methanol / 2 h
2.2: 0.17 h
2.3: 9 h
With
trifluoroacetic acid;
In
methanol; ethanol;
1.1: Ugi condensation / 2.1: Ugi condensation / 2.2: Ugi condensation / 2.3: Ugi condensation;
DOI:10.1021/ja2022027
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / tetrahydrofuran; water / 36 h / 20 °C
2.1: lithium hydroxide / tetrahydrofuran; water / 8 h / 0 - 20 °C
3.1: 2,3,4,5,6-pentafluorophenol; diisopropyl-carbodiimide / dichloromethane / 4 h / 0 - 20 °C
3.2: 20 °C
With
2,3,4,5,6-pentafluorophenol; trifluoroacetic acid; lithium hydroxide; diisopropyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja2022027
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / tetrahydrofuran; water / 36 h / 20 °C
2.1: lithium hydroxide / tetrahydrofuran; water / 8 h / 0 - 20 °C
3.1: 2,3,4,5,6-pentafluorophenol; diisopropyl-carbodiimide / dichloromethane / 4 h / 0 - 20 °C
3.2: 20 °C
4.1: lithium hydroxide / tetrahydrofuran; water / 120 h / 0 - 20 °C
With
2,3,4,5,6-pentafluorophenol; trifluoroacetic acid; lithium hydroxide; diisopropyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja2022027
