N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

Base Information

Chemical Name:N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride
CAS No.:1567842-37-8
Molecular Formula:C₂₂H₂₇ClN₂O*ClH
Molecular Weight:407.383
Hs Code.:

Synonyms:N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

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Chemical Property of N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

Chemical Property:

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Technology Process of N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

There total 5 articles about N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1570522-55-2
N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide

: 1567842-37-8
N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether;
DOI:10.1016/j.bmcl.2014.01.032

Reference yield:

: 1567842-52-7
(E)-N-ethylidene-1-(piperidin-4-yl)methanamine

: 1567842-37-8
N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 12 h / Reflux

2: sodium tetrahydroborate / methanol / 20 °C

3: triethylamine / tetrahydrofuran / 24 h / 0 °C

4: hydrogenchloride / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; acetone;
DOI:10.1016/j.bmcl.2014.01.032

Reference yield:

: 1-(1-benzylpiperidin-4-yl)-N-ethylidenemethanamine

: 1567842-37-8
N-((1-benzylpiperidin-4-yl)methyl)-4-chloro-N-ethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: triethylamine / tetrahydrofuran / 24 h / 0 °C

3: hydrogenchloride / diethyl ether

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/j.bmcl.2014.01.032