O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Base Information

Chemical Name:O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate
CAS No.:1364662-63-4
Molecular Formula:C₄₁H₄₉Cl₃N₄O₁₅
Molecular Weight:944.217
Hs Code.:

O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Synonyms:O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

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Chemical Property of O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

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Technology Process of O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

There total 5 articles about O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate

: 545-06-2
trichloroacetonitrile

: 1364662-63-4
O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1039/c2ob06607f

Reference yield:

: C₄₂H₅₉N₃O₁₄Si

: 1364662-63-4
O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / 36 h / 20 °C

2: pyridine hydrofluoride / tetrahydrofuran / 28 h / -15 - 20 °C / Inert atmosphere

3: potassium carbonate / dichloromethane / 6 h / 20 °C

With pyridine; dmap; pyridine hydrofluoride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob06607f

Reference yield:

: 1380592-26-6
C₄₇H₆₇N₃O₁₅Si

: 1364662-63-4
O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrofluoride / tetrahydrofuran / 28 h / -15 - 20 °C / Inert atmosphere

2: potassium carbonate / dichloromethane / 6 h / 20 °C

With pyridine hydrofluoride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob06607f