C₄₁H₆₆O₄Si₃

Base Information

Chemical Name:C₄₁H₆₆O₄Si₃
CAS No.:1404304-75-1
Molecular Formula:C₄₁H₆₆O₄Si₃
Molecular Weight:707.229
Hs Code.:

C<sub>41</sub>H<sub>66</sub>O<sub>4</sub>Si<sub>3</sub>

Synonyms:C₄₁H₆₆O₄Si₃

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Chemical Property of C₄₁H₆₆O₄Si₃

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Technology Process of C₄₁H₆₆O₄Si₃

There total 12 articles about C₄₁H₆₆O₄Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1404304-74-0
C₃₉H₆₀O₄Si₂

: 15933-59-2
1,1,3,3-tetramethyldisilazane

: 1404304-75-1
C₄₁H₆₆O₄Si₃

Guidance literature:: C₃₉H₆₀O₄Si₂; 1,1,3,3-tetramethyldisilazane; at 50 ℃; for 2.5h; Inert atmosphere;

With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol302409g

Reference yield:

: 102517-37-3
(2R,3R)-1,2-epoxy-3-heptanol

: 1404304-75-1
C₄₁H₆₆O₄Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

4.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

5.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

6.1: triphenylphosphine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -78 - -30 °C / Inert atmosphere

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

8.2: 1.25 h / -78 - 20 °C / Inert atmosphere

9.1: 2.5 h / 50 °C / Inert atmosphere

9.2: 0.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; n-butyllithium; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol302409g

Reference yield:

: 1404304-64-8
C₂₃H₃₂O₂Si

: 1404304-75-1
C₄₁H₆₆O₄Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 1 h / -78 - 20 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 6 h / 40 °C / Inert atmosphere

3.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl) / tetrahydrofuran / 50 °C / Inert atmosphere

4.1: triethylamine / methanol / 0.75 h / 20 °C / Inert atmosphere

5.1: triphenylphosphine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.83 h / -78 - -30 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

7.2: 1.25 h / -78 - 20 °C / Inert atmosphere

8.1: 2.5 h / 50 °C / Inert atmosphere

8.2: 0.5 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; n-butyllithium; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ol302409g