Technology Process of Methyl 4-(5,5-dicyano-4-pentenyl)benzoate
There total 4 articles about Methyl 4-(5,5-dicyano-4-pentenyl)benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
rac-Ala-OH;
In
acetic acid; benzene;
for 3h;
Heating;
DOI:10.1021/jo00297a044
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / palladium chloride, triphenylphosphine, copper(I) iodide, diethylamine / 18 h / Ambient temperature
2: 100 percent / hydrogen / 5percent Pd/C / ethanol / 12 h / 2585.7 Torr
3: 60 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 12 h / Ambient temperature
4: 75 percent / DL-alanine / acetic acid; benzene / 3 h / Heating
With
copper(l) iodide; hydrogen; sodium acetate; diethylamine; triphenylphosphine; rac-Ala-OH; pyridinium chlorochromate; palladium dichloride;
palladium on activated charcoal;
In
ethanol; dichloromethane; acetic acid; benzene;
DOI:10.1021/jo00297a044
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / hydrogen / 5percent Pd/C / ethanol / 12 h / 2585.7 Torr
2: 60 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 12 h / Ambient temperature
3: 75 percent / DL-alanine / acetic acid; benzene / 3 h / Heating
With
hydrogen; sodium acetate; rac-Ala-OH; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; acetic acid; benzene;
DOI:10.1021/jo00297a044
