1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

Base Information

Chemical Name:1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine
CAS No.:1298071-99-4
Molecular Formula:C₂₄H₂₃NO₇
Molecular Weight:437.449
Hs Code.:

Synonyms:1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

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Technology Process of 1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

There total 3 articles about 1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 22216-25-7
1-(3,5-dimethoxybenzyloxy)-3,5-dimethoxybenzene

: 555-16-8
4-nitrobenzaldehdye

: 1298071-99-4
1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201001739

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 1298071-99-4
1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001739

Reference yield:

: 877-88-3
3,5-dimethoxybenzyl bromide

: 1298071-99-4
1,3,8,10-tetramethoxy-11-(4-nitrophenyl)-6,11-dihydrodibenzo[b,e]oxepine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201001739