amminepentacarbonylmolybdenum

Base Information

Chemical Name:amminepentacarbonylmolybdenum
CAS No.:13931-12-9
Molecular Formula:C₅H₃MoNO₅
Molecular Weight:253.023
Hs Code.:

Synonyms:amminepentacarbonylmolybdenum

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of amminepentacarbonylmolybdenum

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Technology Process of amminepentacarbonylmolybdenum

There total 1 articles about amminepentacarbonylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 53248-43-4
pentacarbonyl(tetrahydrofuran)molybdenum⁽⁰⁾

: 117696-62-5
C₄H₄B(C₆H₅)(NH₃)

: 13931-12-9
amminepentacarbonylmolybdenum

: tetracarbonyl{η5-(1-phenylborole)}molybdenum

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

Guidance literature:: In tetrahydrofuran; under N2, to soln. of Mo(CO)5(THF) in THF added soln. of C4H4B(Ph)(NH3) in THF, kept at 65°C for 5 h; evapd.(vac.), extd.(pentane), filtered, concd., cooled(-30°C), chromd. (Al2O3/7% H2O(water-cooled, light protected column); pentane, pentane/ether), concd.(vac.), dried(1E-5 bar/-78°C), sublimed(1E-5 bar), crystd.(hexane); elem. anal.;
DOI:10.1016/0022-328X(87)87155-3