C₂₇H₂₈N₂O₉

Base Information

Chemical Name:C₂₇H₂₈N₂O₉
CAS No.:1315454-89-7
Molecular Formula:C₂₇H₂₈N₂O₉
Molecular Weight:524.527
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₂₇H₂₈N₂O₉

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Chemical Property of C₂₇H₂₈N₂O₉

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Technology Process of C₂₇H₂₈N₂O₉

There total 28 articles about C₂₇H₂₈N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1315454-86-4
C₂₉H₃₀N₂O₁₀

: 1315454-89-7
C₂₇H₂₈N₂O₉

: 1315454-87-5
C₂₇H₂₈N₂O₉

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at 78 ℃; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield: 52.0%

: 1315454-85-3
C₂₇H₂₈N₂O₈

: 1315454-89-7
C₂₇H₂₈N₂O₉

Guidance literature:: C₂₇H₂₈N₂O₈; With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With acetic anhydride; In tetrahydrofuran; at -15 ℃; for 34h; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 163495-25-8
3-Benzyloxy-4-iodo-5-nitro-benzoic acid methyl ester

: 1315454-89-7
C₂₇H₂₈N₂O₉

Guidance literature:: Multi-step reaction with 11 steps

1: iron; acetic acid / tetrahydrofuran; methanol / 3.5 h / 20 °C / Inert atmosphere

2: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

3: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

5: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

6: 1,4-diaza-bicyclo[2.2.2]octane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine / tetrahydrofuran / 20 °C / Inert atmosphere

7: palladium diacetate; silver nitrate; triphenylphosphine / 1,4-dioxane / 1 h / 80 °C / Inert atmosphere

8: 4-methyl-morpholine; osmium(VIII) oxide / tetrahydrofuran; water; acetone / 3 h / 20 °C / Inert atmosphere

9: pyridine / dichloromethane / 0.08 h / -78 - 0 °C / Inert atmosphere

10: tetrahydrofuran / 24 h / -20 - 0 °C / Inert atmosphere

11: methanol; sodium methylate / tetrahydrofuran / 78 °C / Inert atmosphere

With 4-methyl-morpholine; pyridine; 1,4-diaza-bicyclo[2.2.2]octane; methanol; dmap; osmium(VIII) oxide; bis(1,5-cyclooctadiene)diiridium(I) dichloride; tetrabutyl ammonium fluoride; sodium methylate; palladium diacetate; iron; sodium cyanoborohydride; potassium carbonate; silver nitrate; acetic acid; triphenylphosphine; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetone; 9: Polonovski reaction;
DOI:10.1002/chem.201003489