Technology Process of BEt-3IP
There total 7 articles about BEt-3IP which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H29NO3;
With
water; sodium hydroxide;
In
methanol;
at 60 ℃;
for 1h;
With
hydrogenchloride; water;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
3.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 110 °C / Reflux; Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere
4.2: 0.08 h / 20 °C / Inert atmosphere
5.1: water; sodium hydroxide / methanol / 1 h / 60 °C
With
hydrogenchloride; water; hydrogen; sodium hydride; potassium carbonate; caesium carbonate; potassium iodide; sodium hydroxide;
tris-(dibenzylideneacetone)dipalladium(0); palladium on activated charcoal; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
methanol; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid; water; sodium nitrite / 0 - 5 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
3.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
4.1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 110 °C / Reflux; Inert atmosphere
5.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere
5.2: 0.08 h / 20 °C / Inert atmosphere
6.1: water; sodium hydroxide / methanol / 1 h / 60 °C
With
hydrogenchloride; sulfuric acid; water; hydrogen; sodium hydride; potassium carbonate; caesium carbonate; potassium iodide; sodium hydroxide; sodium nitrite;
tris-(dibenzylideneacetone)dipalladium(0); palladium on activated charcoal; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
methanol; water; N,N-dimethyl-formamide; toluene;
