HYDROGEN PHOSPHATE IONOPHORE I

Base Information

• Chemical Name: HYDROGEN PHOSPHATE IONOPHORE I
• CAS No.: 32065-17-1
• Molecular Formula: C₂₀H₁₄N₂O₃V
• Molecular Weight: 381.284
• Mol file: 32065-17-1.mol

Synonyms:Vanadium,oxo[[2,2'-[1,2-phenylenebis(nitrilomethylidyne)]bis[phenolato]](2-)-N,N',O,O']-,(SP-5-23)-; Vanadium, oxo[[a,a'-(o-phenylenedinitrilo)di-o-cresolato](2-)]-(8CI); Phenol, 2,2'-[1,2-phenylenebis(nitrilomethylidyne)]bis-, vanadiumcomplex; Oxo(bis(salicylidene)-o-phenylenediaminato)vanadium; [Bis(salicylidene)-o-phenylenediamine]oxovanadium

Chemical Property of HYDROGEN PHOSPHATE IONOPHORE I

Chemical Property:

• PSA: 58.20000
• LogP: 3.69560
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

N,N′-Bis(salicylidene)-o-phenylenediamine Vanadium(IV) oxide Complex ≥98.0% (HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HYDROGEN PHOSPHATE IONOPHORE I

There total 10 articles about HYDROGEN PHOSPHATE IONOPHORE I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

vanadium trisacetylacetonate + (E)-N,N'-bis(salicylidene)-1,2-phenylenediamine (3946-91-6,86328-88-3) → vanadyl N,N'-phenylenebis(salicylideneiminato) (32065-17-1,335151-29-6)

Guidance literature:

With oxygen; In methanol; at 20 ℃;

DOI:10.1016/j.cattod.2012.03.032

Reference yield: 73.0%

tris(acetylacetonato)vanadium(III) (13476-99-8) + N,N'-bis(salicylidene)-o-phenylenediamine (3946-91-6) → vanadyl N,N'-phenylenebis(salicylideneiminato) (32065-17-1,335151-29-6)

Guidance literature:

With oxygen; In methanol; at 20 ℃;

DOI:10.1016/j.cattod.2012.03.032

Reference yield:

vanadyl(IV) sulphate pentahydrate + (E)-N,N'-bis(salicylidene)-1,2-phenylenediamine (3946-91-6,86328-88-3) → vanadyl N,N'-phenylenebis(salicylideneiminato) (32065-17-1,335151-29-6)

Guidance literature:

In ethanol; water; at 80 ℃;

DOI:10.1016/j.molcata.2016.05.016

upstream raw materials:

bis(acetylacetonate)oxovanadium

N,N'-bis(salicylidene)-o-phenylenediamine

{V(OMe)2(salphen)}

water

Downstream raw materials:

2VO⁽²⁺⁾*2OC₆H₄CHNC₆H₄NCHC₆H₄O^(2-)*Na⁽¹⁺⁾*B(C₆H₅)4^(1-)=[(VO(OC₆H₄CHNC₆H₄NCHC₆H₄O))2Na]B(C₆H₅)4

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