9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine

Base Information

• Chemical Name: 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine
• CAS No.: 957781-51-0
• Molecular Formula: C₉₀H₆₀N₈
• Molecular Weight: 1253.52
• Mol file: 957781-51-0.mol

Synonyms:9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine

Chemical Property of 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine

There total 1 articles about 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9-(4-nitrophenyl)carbazole-3,6-diamine → 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine (957781-51-0)

Guidance literature:

With tin(ll) chloride; In ethanol; for 48h; Heating;

DOI:10.1021/ol702060u

Reference yield: 60.0%

9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine (957781-51-0) + 1-bromo-4-tert-butylbenzene (3972-65-4) → 9-[4-(4-tert-butylphenylamino)phenyl]-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine

Guidance literature:

With tri-tert-butyl phosphine; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; for 16h; Heating;

DOI:10.1021/ol702060u

Reference yield: 46.0%

trifluoromethanesulfonic acid 4-{3,6-bis[bis(4-carbazol-9-yl-phenyl)amino]-carbazol-9-yl}phenyl ester + 9-(4-aminophenyl)-N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-9H-carbazole-3,6-diamine (957781-51-0) → 4-{3,6-bis[bis(4-carbazol-9-yl-phenyl)amino]-carbazol-9-yl}phenol + bis-{N,N,N',N'-tetrakis(4-carbazol-9-yl-phenyl)-[4-(3,6-diaminocarbazol-9-yl)phenyl]}amine

Guidance literature:

With johnphos; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In o-xylene; for 72h; Heating;

DOI:10.1021/ol702060u

Downstream raw materials:

C₁₂₀H₈₈N₁₂O₂