1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

Base Information

Chemical Name:1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane
CAS No.:86042-99-1
Molecular Formula:C₁₇H₁₅F₃O
Molecular Weight:292.301
Hs Code.:

Synonyms:1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

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Chemical Property of 1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

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Technology Process of 1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

There total 12 articles about 1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 402-43-7
p-trifluoromethylphenyl bromide

: 5-(1-(4-methoxyphenyl)cyclopropyl)-1-aza-5-germabicyclo[3.3.3]undecane

: 86042-99-1
1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

Guidance literature:: With bis(3,5-bis(trifluoromethyl)phenyl)(2-(2,4,6-triisopropylphenyl)-1H-inden-3-yl)phosphine; copper(l) chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 100 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1039/d1cc02930d

Reference yield: 45.0%

: O-(1-(4-(trifluoromethyl)phenyl)cyclopropyl) benzoyl(phenyl)carbamothioate

: 4-methoxyphenylzinc(II) methoxide

: 86042-99-1
1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

Guidance literature:: O-(1-(4-(trifluoromethyl)phenyl)cyclopropyl) benzoyl(phenyl)carbamothioate; With nickel(II) acetylacetonate monohydrate; Bathocuproine; magnesium chloride; In 1,4-dioxane; at 23 ℃; for 0.0833333h; Inert atmosphere; Sealed tube;

4-methoxyphenylzinc(II) methoxide; In tetrahydrofuran; 1,4-dioxane; at 23 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.0c06904

Reference yield:

: 1,3-dioxoisoindolin-2-yl 1-(4-methoxyphenyl)cyclopropane-1-carboxylate

: 86042-99-1
1-(p-methoxyphenyl)-1-(p-(trifluoromethyl)phenyl)cyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: zinc / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere; Sealed tube

2: bis(3,5-bis(trifluoromethyl)phenyl)(2-(2,4,6-triisopropylphenyl)-1H-inden-3-yl)phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; copper(l) chloride / tetrahydrofuran / 16 h / 100 °C / Inert atmosphere; Sealed tube

With bis(3,5-bis(trifluoromethyl)phenyl)(2-(2,4,6-triisopropylphenyl)-1H-inden-3-yl)phosphine; copper(l) chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; zinc; In tetrahydrofuran;
DOI:10.1039/d1cc02930d