2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

Base Information

Chemical Name:2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt
CAS No.:1612163-61-7
Molecular Formula:C₂H₂O₄*C₁₄H₂₁BrN₂O₂
Molecular Weight:419.272
Hs Code.:

Synonyms:2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

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Chemical Property of 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

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Technology Process of 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

There total 2 articles about 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 76790-28-8,127896-05-3
N-<(4-Bromophenyl)methylene>-2-methyl-2-propanamine N-oxide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1612163-61-7
2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

Guidance literature:: With lithium 2,2,6,6-tetramethylpiperidide; In tetrahydrofuran; toluene; at -78 ℃; for 0.333333h;
DOI:10.1021/jo500848a

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1612163-61-7
2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylacetamide oxalic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / dichloromethane / 20 °C

2: lithium 2,2,6,6-tetramethylpiperidide / toluene; tetrahydrofuran / 0.33 h / -78 °C

With lithium 2,2,6,6-tetramethylpiperidide; sodium carbonate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo500848a