C₂₅H₂₅NO

Base Information

Chemical Name:C₂₅H₂₅NO
CAS No.:1620092-66-1
Molecular Formula:C₂₅H₂₅NO
Molecular Weight:355.48
Hs Code.:

Synonyms:C₂₅H₂₅NO

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Chemical Property of C₂₅H₂₅NO

Chemical Property:

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Technology Process of C₂₅H₂₅NO

There total 4 articles about C₂₅H₂₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 624-31-7
4-tolyl iodide

: C₂₆H₃₂BNO

: 1620092-66-1
C₂₅H₂₅NO

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide; In water; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja506310v

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1620092-66-1
C₂₅H₂₅NO

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / 60 °C / Inert atmosphere; Sealed tube

2: tributylphosphine / tetrahydrofuran / 8 h / 80 °C / Inert atmosphere; Sealed tube

3: tetrahydrofuran; methanol / 24 h / 60 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / water / 24 h / 120 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; water; 4: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja506310v

Reference yield:

: 67753-90-6
B-2-phenylethyl-9-BBN

: 1620092-66-1
C₂₅H₂₅NO

Guidance literature:: Multi-step reaction with 3 steps

1: tributylphosphine / tetrahydrofuran / 8 h / 80 °C / Inert atmosphere; Sealed tube

2: tetrahydrofuran; methanol / 24 h / 60 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / water / 24 h / 120 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; water; 3: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja506310v