Technology Process of C32H44O4
There total 9 articles about C32H44O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
In
dichloromethane; acetonitrile;
at 20 ℃;
for 1h;
DOI:10.1021/jm300566h
- Guidance literature:
-
With
mercury(II) perchlorate hexahydrate;
In
dichloromethane; water; acetonitrile;
at 4 ℃;
for 1h;
DOI:10.1021/jm300566h
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / 20 °C / Inert atmosphere
1.2: 2 h / 4 °C / Inert atmosphere
2.1: pyridinium p-toluenesulfonate / methanol / 17 h / 20 °C
3.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 20 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Molecular sieve
5.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
6.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C
7.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C
With
n-butyllithium; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; camphor-10-sulfonic acid; water; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; acetonitrile;
DOI:10.1021/jm300566h
