C₃₅H₆₉N₂O₇PSi

Base Information

Chemical Name:C₃₅H₆₉N₂O₇PSi
CAS No.:1236062-62-6
Molecular Formula:C₃₅H₆₉N₂O₇PSi
Molecular Weight:689.001
Hs Code.:

C<sub>35</sub>H<sub>69</sub>N<sub>2</sub>O<sub>7</sub>PSi

Synonyms:C₃₅H₆₉N₂O₇PSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₆₉N₂O₇PSi

Chemical Property:

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Technology Process of C₃₅H₆₉N₂O₇PSi

There total 11 articles about C₃₅H₆₉N₂O₇PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1236062-73-9
C₃₁H₆₀N₂O₄Si

: 814-49-3
diethyl chlorophosphate

: 1236062-62-6
C₃₅H₆₉N₂O₇PSi

Guidance literature:: With 1-methyl-1H-imidazole; In tetrahydrofuran; at 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ja104250b

Reference yield:

: 1236062-70-6
(8S)-triisopropylsilyloxy-1-(tert-butyldimethylsiloxy)dodec-6-yn-5-ol

: 1236062-62-6
C₃₅H₆₉N₂O₇PSi

Guidance literature:: Multi-step reaction with 8 steps

2: (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); isopropyl alcohol

3: platinum(IV) oxide; hydrogen

4: methanol; pyridinium p-toluenesulfonate

5: bromine; triethylamine; triphenylphosphine

6: lithium diisopropyl amide / tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / -78 - 0 °C

7: methanol; pyridinium p-toluenesulfonate

8: 1-methyl-1H-imidazole

With 1-methyl-1H-imidazole; methanol; platinum(IV) oxide; (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); hydrogen; bromine; pyridinium p-toluenesulfonate; triethylamine; triphenylphosphine; isopropyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 1: Swern oxidation;
DOI:10.1021/jo300161x

Reference yield:

: 1236062-57-9
(8S)-triisopropylsilyloxy-1-(tert-butyldimethylsilyloxy)dodec-6-yn-5-one

: 1236062-62-6
C₃₅H₆₉N₂O₇PSi

Guidance literature:: Multi-step reaction with 7 steps

1: (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); isopropyl alcohol

2: platinum(IV) oxide; hydrogen

3: methanol; pyridinium p-toluenesulfonate

4: bromine; triethylamine; triphenylphosphine

5: lithium diisopropyl amide / tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / -78 - 0 °C

6: methanol; pyridinium p-toluenesulfonate

7: 1-methyl-1H-imidazole

With 1-methyl-1H-imidazole; methanol; platinum(IV) oxide; (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); hydrogen; bromine; pyridinium p-toluenesulfonate; triethylamine; triphenylphosphine; isopropyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone;
DOI:10.1021/jo300161x