bis(α,2-dihydroxybenzyl)phenylphosphine oxide

Base Information

Chemical Name:bis(α,2-dihydroxybenzyl)phenylphosphine oxide
CAS No.:125300-94-9
Molecular Formula:C₂₀H₁₉O₅P
Molecular Weight:370.342
Hs Code.:

Synonyms:bis(α,2-dihydroxybenzyl)phenylphosphine oxide

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Chemical Property of bis(α,2-dihydroxybenzyl)phenylphosphine oxide

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Technology Process of bis(α,2-dihydroxybenzyl)phenylphosphine oxide

There total 1 articles about bis(α,2-dihydroxybenzyl)phenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 90-02-8
salicylaldehyde

: 638-21-1
phenylphosphane

: 125300-94-9
bis(α,2-dihydroxybenzyl)phenylphosphine oxide

Guidance literature:: With dihydrogen peroxide; In acetone;
DOI:10.1007/BF00953306

Reference yield: 23.0%

: 3262-89-3
triphenylboroxine

: 102-82-9
tributyl-amine

: 125300-94-9
bis(α,2-dihydroxybenzyl)phenylphosphine oxide

: tributylammonium 1,4-diphenyl-4-oxo-3-(o-hydroxyphenyl)-2,8,9-trioxa-1-borata-6,7-benzobicyclo{3.3.1}non-6-ene

Guidance literature:: With pyridine; In acetone; under Ar, addn. of pyridine and phenylboric anhydride to phosphine oxide, heating, 2 h, evapn. of excess pyridine, addn. of tributylamine in acetone; evapn. of solvent in vac., crystn. from acetone-ether (3:1); elem. anal.;
DOI:10.1007/BF00953306

Reference yield: 20.0%

: 23147-97-9
isobutyl diphenylborinate

: 125300-94-9
bis(α,2-dihydroxybenzyl)phenylphosphine oxide

: bis(triethylammonium 2,2-diphenyl-5,6-benzo-1,3,2-dioxaborin-4-yl)phenylphosphine oxide

Guidance literature:: With triethylamine; In triethylamine; under Ar; evapn. of excess Et3N in vac., crystn. from acetone-ether (3:1); elem. anal.;
DOI:10.1007/BF00953306