5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

Base Information

Chemical Name:5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione
CAS No.:152450-71-0
Molecular Formula:C₁₅H₂₁N₃OS
Molecular Weight:291.417
Hs Code.:

Synonyms:5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

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Chemical Property of 5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

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Technology Process of 5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

There total 1 articles about 5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 97481-71-5
1,2,2,5,5-pentamethyl-2,5-dihydro-1H-imidazole 3-oxide

: 103-72-0
phenyl isothiocyanate

: 152450-71-0
5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

Guidance literature:: In chloroform; for 48h;
DOI:10.1007/BF00863378

Reference yield: 98.0%

: 152450-71-0
5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

: 152450-75-4
1,2,2,5,5-pentamethyl-4-(N-phenylimino)-3-imidazoline

Guidance literature:: With sodium hydroxide; In ethanol;
DOI:10.1007/BF00863378

Reference yield:

: 152450-71-0
5,5,6,7,7-Pentamethyl-1-phenyl-tetrahydro-imidazo[1,5-b][1,2,4]oxadiazole-2-thione

: C₁₆H₂₆N₃⁽¹⁺⁾*CH₃O₄S^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / aq. NaOH / ethanol

2: Na₂CO₃ / CHCl₃ / 72 h

With sodium hydroxide; sodium carbonate; In ethanol; chloroform;
DOI:10.1007/BF00863378