Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇

Base Information

• Chemical Name: Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇
• CAS No.: 947494-23-7
• Molecular Formula: C₃₁H₃₇N₃O₄*C₁₂₃H₁₅₀N₄O₇Pd
• Molecular Weight: 2418.64

Synonyms:Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇

Chemical Property of Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇

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Technology Process of Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇

There total 1 articles about Pd(C₅H₃N(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₅H₁₀)2)*N₃C₃₁O₄H₃₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Pd(NC5H3(CH2OC6H4C(C6H4C(CH3)3)3)(CH2O(CH2)11OC6H4C(C6H4C(CH3)3)3))(NC5H3(CONCH2C6H4OC4H8CHCH2)2)*C31N3O4H37 (947494-22-6) → Pd(C5H3N(CH2OC6H4C(C6H4C(CH3)3)3)(CH2O(CH2)11OC6H4C(C6H4C(CH3)3)3))(NC5H3(CONCH2C6H4OC5H10)2)*N3C31O4H37 (947494-23-7)

Guidance literature:

With triethylamine; Grubbs catalyst first generation; In dichloromethane; under N2; soln. of Pd-complex in CH2Cl2 added to soln. of Grubbs catalyst, soln. stirred at room temp. for 18 h, concd. under vac., column chromy., dissolved in CH2Cl2, hydrazide and Et3N added, mixt. stirred overnight; soln. washed with NaHCO3, org. layers combined, concd.;

DOI:10.1002/anie.200700933

upstream raw materials:

Pd(NC₅H₃(CH₂OC₆H₄C(C₆H₄C(CH₃)3)3)(CH₂O(CH₂)11OC₆H₄C(C₆H₄C(CH₃)3)3))(NC₅H₃(CONCH₂C₆H₄OC₄H₈CHCH₂)2)*C₃₁N₃O₄H₃₇

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