F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃

Base Information

• Chemical Name: F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃
• CAS No.: 116025-52-6
• Molecular Formula: C₁₆H₁₁BF₂O₃Te
• Molecular Weight: 427.669

Synonyms:F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃

Chemical Property of F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃

Chemical Property:

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Technology Process of F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃

There total 1 articles about F₂BO₂C₃H(C₆H₅)Te(C₆H₂)OCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

boron trifluoride (7637-07-2) + 4H-2-phenyl-5,7-dimethoxybenzotelluropyrone (84144-55-8) → F2BO2C3H(C6H5)Te(C6H2)OCH3 (116025-52-6)

Guidance literature:

In diethyl ether; Dissolving of organotellurium-complex in distilled BF3 etherate, heating of resulting soln. on a steam bath (1 h).; Diluting of react. mixt. with ether, filtn. and recrystn. from CH3CN gives boronate compd. Elem. anal.;

Reference yield: 90.0%

F2BO2C3H(C6H5)Te(C6H2)OCH3 (116025-52-6) → 2-phenyl-5-hydroxy-7-methoxybenzo{b}tellurapyranone (116006-74-7)

Guidance literature:

With potassium carbonate; In water; acetone; Slurring of boronate compd. with K2CO3 in acetone and H2O, heating of resulting mixt. at reflux.; Acidifying of react. mixt. (HCl), filtn., recrystn. from methanol.;

upstream raw materials:

boron trifluoride

4H-2-phenyl-5,7-dimethoxybenzotelluropyrone

Downstream raw materials:

2-phenyl-5-hydroxy-7-methoxybenzo{b}tellurapyranone

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