benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester

Base Information

• Chemical Name: benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester
• CAS No.: 125760-09-0
• Molecular Formula: C₉₂H₉₇F₅N₆O₂₁
• Molecular Weight: 1717.8

Synonyms:benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester

Chemical Property of benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester

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Technology Process of benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester

There total 1 articles about benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2,3,4,5,6-pentafluorophenol (771-61-9) + benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid → benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester (125760-09-0)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1016/0040-4020(95)00964-7

Reference yield: 24.0%

benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester (125760-09-0) → Cyclo-(D-Ala-L-Hyhc-L-Val-D-Hyhc)3 (125760-10-3)

Guidance literature:

With dmap; hydrogen; palladium on activated charcoal; In 1,4-dioxane; at 90 ℃; for 48h;

DOI:10.1016/S0040-4039(00)99557-1

Reference yield: 24.0%

benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamic acid pentafluorophenyl ester (125760-09-0) → cyclo D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxyhydrocinnamyl D-alanyl L-α-hydroxycinnamyl L-valyl D-α-hydroxyhydrocinnamyl

Guidance literature:

With dmap; hydrogen; palladium on activated charcoal; In 1,4-dioxane; ethanol; at 92 ℃;

DOI:10.1016/0040-4020(95)00964-7

upstream raw materials:

2,3,4,5,6-pentafluorophenol

Downstream raw materials:

Cyclo-(D-Ala-L-Hyhc-L-Val-D-Hyhc)3

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