3'-methoxy-deoxybenzoin oxime

Base Information

• Chemical Name: 3'-methoxy-deoxybenzoin oxime
• CAS No.: 119513-95-0
• Molecular Formula: C₁₅H₁₅NO₂
• Molecular Weight: 241.29
• Mol file: 119513-95-0.mol

Synonyms:3'-methoxy-deoxybenzoin oxime

Chemical Property of 3'-methoxy-deoxybenzoin oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3'-methoxy-deoxybenzoin oxime

There total 4 articles about 3'-methoxy-deoxybenzoin oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1′-(3-methoxyphenyl)-2′-phenylethan-2′-one (29955-26-8) → 3'-methoxy-deoxybenzoin oxime (119513-95-0)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; water;

Reference yield:

methyl-(α'-nitro-stilben-3-yl)-ether (50882-22-9) → 3'-methoxy-deoxybenzoin oxime (119513-95-0)

Guidance literature:

With pyridine; palladium on activated charcoal; at 50 - 60 ℃; Hydrogenation;

DOI:10.1002/ardp.19362740301

Reference yield:

1-nitro-1-phenylmethane (622-42-4) → 3'-methoxy-deoxybenzoin oxime (119513-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂CO₃; ethanol

2: pyridine; palladium/charcoal / 50 - 60 °C / Hydrogenation

With pyridine; palladium on activated charcoal; ethanol; sodium carbonate;

DOI:10.1002/ardp.19362740301

upstream raw materials:

methyl-(α'-nitro-stilben-3-yl)-ether

1-nitro-1-phenylmethane

3-methoxy-benzaldehyde

1′-(3-methoxyphenyl)-2′-phenylethan-2′-one

Downstream raw materials:

dl-2-(3-methoxyphenyl)-1-phenylethylamine hydrochloride