((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

Base Information

Chemical Name:((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide
CAS No.:1242097-23-9
Molecular Formula:C₃₈H₄₆O₂P*I
Molecular Weight:692.66
Hs Code.:

Synonyms:((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

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Chemical Property of ((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

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Technology Process of ((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

There total 1 articles about ((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1242097-53-5
1-((((5R,6S)-10-iodo-2,6-dimethyldec-2-en-5-yl)oxy)methyl)-4-methoxybenzene

: 603-35-0
triphenylphosphine

: 1242097-23-9
((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

Guidance literature:: In toluene; for 14h; Reflux; Darkness; Inert atmosphere;
DOI:10.1021/ol101843q

Reference yield: 63.0%

: 590-97-6
acetoxymethyl bromide

: 1242097-22-8
(E)-6-((4-methoxybenzyl)oxy)-4-methylhex-4-enal

: 1242097-23-9
((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide

: 1242097-28-4
(6S,7R,Z)-7-((4-methoxybenzyl)oxy)-2-((E)-6-((4-methoxybenzyl)oxy)-4-methylhex-4-en-1-ylidene)-6,10-dimethylundec-9-en-1-yl acetate

Guidance literature:: ((5S,6R)-6-((4-methoxybenzyl)oxy)-5,9-dimethyldec-8-en-1-yl)triphenylphosphonium iodide; With lithium bromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

With phenyllithium; In tetrahydrofuran; dibutyl ether; at -78 - 20 ℃; for 0.75h; Inert atmosphere;

acetoxymethyl bromide; (E)-6-((4-methoxybenzyl)oxy)-4-methylhex-4-enal; Further stages;
DOI:10.1021/ol101843q