Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]

Base Information

• Chemical Name: Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]
• CAS No.: 220528-58-5
• Molecular Formula: Br₄Pd*C₆₈H₆₆O₂P₆Pd
• Molecular Weight: 1633.57
• Mol file: 220528-58-5.mol

Synonyms:Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]

Chemical Property of Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄]

There total 2 articles about Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2⁽²⁺⁾*PdBr₄^(2-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(O)(C₆H₅)2)2][PdBr₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br(1+)*Br(1-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(C6H5)2)Br]Br (220528-51-8) → Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(O)(C6H5)2)2(2+)*PdBr4(2-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(O)(C6H5)2)2][PdBr4] (220528-58-5)

Guidance literature:

With H₂O₂; In diethyl ether; acetone; evapn., washing (ethanol), drying; elem. anal.;

DOI:10.1016/S0277-5387(98)00307-6

Reference yield:

bis(2-diphenylphosphinoethyl)phenylphosphine (23582-02-7) → Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(O)(C6H5)2)2(2+)*PdBr4(2-)=[Pd((C6H5)2P(CH2)2P(C6H5)(CH2)2P(O)(C6H5)2)2][PdBr4] (220528-58-5)

Guidance literature:

Multi-step reaction with 2 steps

1: water; dichloromethane

2: H₂O₂ / acetone; diethyl ether

With H₂O₂; In diethyl ether; dichloromethane; water; acetone;

DOI:10.1016/S0277-5387(98)00307-6

upstream raw materials:

Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br⁽¹⁺⁾*Br^(1-)=[Pd((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)2P(C₆H₅)2)Br]Br

bis(2-diphenylphosphinoethyl)phenylphosphine