Technology Process of C32H50N2O6Si
There total 6 articles about C32H50N2O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; titanium(III) chloride; sodium acetate; zinc;
In
methanol; dichloromethane;
Inert atmosphere;
DOI:10.1002/asia.200800382
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / -40 °C
1.2: 5 h / -40 - 0 °C
2.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C
3.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere
With
hydrogenchloride; titanium(III) chloride; sodium acetate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/chem.201101058
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C
2: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere
With
hydrogenchloride; titanium(III) chloride; sodium acetate; potassium carbonate; zinc;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/chem.201101058