methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

Base Information

Chemical Name:methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate
CAS No.:91632-80-3
Molecular Formula:C₂₀H₂₁NO₃
Molecular Weight:323.392
Hs Code.:

Synonyms:methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

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Chemical Property of methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

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Technology Process of methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

There total 3 articles about methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91632-75-6
N-methyl-N-(3,5-dimethylphenyl)hydrazone of methyl 4-phenyl-2-oxo-3-butenoate

: 91632-80-3
methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

Guidance literature:: With PPA; Polyphosphoric acid (PPA); at 110 ℃; for 0.25h;
DOI:10.1021/jo00197a009

Reference yield:

: 107969-78-8
methyl benzylidenepyruvate

: 91632-80-3
methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / methanol / Heating

2: 0.58 g / polyphosphoric acid (PPA) / 0.25 h / 110 °C

With PPA; Polyphosphoric acid (PPA); acetic acid; In methanol;
DOI:10.1021/jo00197a009

Reference yield:

: 80398-80-7
N-methyl N-(3,5-dimethylphenyl)hydrazine

: 91632-80-3
methyl 3-<2,4-dimethyl-6-(methylamino)phenyl>-3-oxo-4-phenyl-3-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / methanol / Heating

2: 0.58 g / polyphosphoric acid (PPA) / 0.25 h / 110 °C

With PPA; Polyphosphoric acid (PPA); acetic acid; In methanol;
DOI:10.1021/jo00197a009