9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

Base Information

Chemical Name:9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide
CAS No.:651055-75-3
Molecular Formula:C₂₆H₂₀N₄O₈S₂
Molecular Weight:580.599
Hs Code.:

Synonyms:9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

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Chemical Property of 9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

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Technology Process of 9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

There total 2 articles about 9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: N,N'-bis(3-hydroxyphenyl)-9,10-dioxo-9,10-dihydro-2,7-anthracenedisulfonamide

: 651055-71-9
10-(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9-oxo-9,10-dihydro-2,7-anthracenedisulfonamide

: 651055-75-3
9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

Guidance literature:: With hydroxylamine hydrochloride; In methanol; for 18h; Heating / reflux;

Reference yield:

: 853-67-8,10017-59-1
anthraquinone-2,7-disulphonic acid disodium salt

: 651055-71-9
10-(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9-oxo-9,10-dihydro-2,7-anthracenedisulfonamide

: 651055-75-3
9,10-bis(hydroxyimino)-N,N'-bis(3-hydroxyphenyl)-9,10-dihydro-2,7-anthracenedisulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / sulfolane; acetonitrile / 20 h / Heating / reflux

2: pyridine / dichloromethane / 18 h / 20 °C

3: hydroxylamine hydrochloride / methanol / 18 h / Heating / reflux

With pyridine; hydroxylamine hydrochloride; trichlorophosphate; In sulfolane; methanol; dichloromethane; acetonitrile;