Technology Process of C20H24N7O4P
There total 8 articles about C20H24N7O4P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
phosphonic acid diethyl ester;
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
C16H14BrN7O;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate; sodium iodide / acetone / 18 h / 20 °C
2.1: ammonia / tetrahydrofuran; methanol / 2 h / 20 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
4.1: 0.75 h / 80 °C
5.1: iron; acetic acid / water / 64 h / 20 °C
6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 4 h / 0 - 20 °C / Inert atmosphere
7.1: acetic acid; hydrogen bromide / 1 h / 20 °C
8.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C
8.2: 16 h / 20 °C
With
ammonia; hydrogen bromide; iron; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: iron; acetic acid / water / 64 h / 20 °C
2.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 4 h / 0 - 20 °C / Inert atmosphere
3.1: acetic acid; hydrogen bromide / 1 h / 20 °C
4.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C
4.2: 16 h / 20 °C
With
hydrogen bromide; iron; sodium hydride; diisobutylaluminium hydride; acetic acid;
In
tetrahydrofuran; water; toluene;
