4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane
CAS No.:1350934-27-8
Molecular Formula:C₁₆H₂₇BO₂Si
Molecular Weight:290.286
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

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Technology Process of 4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

There total 2 articles about 4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 696-62-8
para-iodoanisole

: C₂₂H₃₈B₂O₄Si

: (1-(4-methoxyphenyl)vinyl)dimethyl(phenyl)silane

: 1350934-27-8
4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

Guidance literature:: With palladium(II) trifluoroacetate; C₄₀H₄₀F₁₂FeP₂; sodium methylate; sodium iodide; In 1,4-dioxane; at 20 ℃; for 3h; enantioselective reaction;
DOI:10.1021/acscatal.8b03979

Reference yield: 21.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1350934-31-4
5-ethyl-5,6-dihydrobenzo[e]pyrazolo[1,5-c][1,3,2]diazaborinine

: 766-77-8
Dimethylphenylsilane

: 1350934-27-8
4,4,5,5-tetramethyl-2-[1-(dimethylphenylsilyl)ethyl]-1,3,2-dioxaborolane

: 200010-93-1
dimethyl(phenyl)(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethyl)silane

Guidance literature:: With norbornene; anisole; carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; boron compd., RuH2(CO)(PPh3)3, norbornene, silane and anisol in toluene heated (135°C, 36 h), treated with pinacol and TsOH in THF at room temp. for 1 h; NMR;
DOI:10.1246/cl.2011.916