tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

Base Information

Chemical Name:tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate
CAS No.:1421349-03-2
Molecular Formula:C₂₆H₃₂N₂O₂
Molecular Weight:404.552
Hs Code.:

Synonyms:tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

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Chemical Property of tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

Chemical Property:

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Technology Process of tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

There total 4 articles about tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1873-55-8
3-methylquinoline N-oxide

: 1421349-02-1
(+/-)-tert-butyl 4-(1-amino-3-methylbutyl)benzoate

: 1421349-03-2
tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 612-58-8
3-methylquinoline

: 1421349-03-2
tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; acetic acid / water / 16 h / 80 °C

2: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

With dihydrogen peroxide; acetic acid; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; water;

Reference yield:

: 1266998-03-1
4-(3-methylbutanoyl)benzoic acid

: 1421349-03-2
tert-butyl (+/-)-4-(3-methyl-1-((3-methylquinolin-2-yl)amino)butyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 50 h / 20 °C

2: sodium cyanoborohydride; ammonium acetate / methanol / 21 h / 60 °C

3: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

With ammonium acetate; sodium cyanoborohydride; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In methanol; dichloromethane;