4-Iodo-2-Methoxy-1-nitrobenzene

Base Information

• Chemical Name: 4-Iodo-2-Methoxy-1-nitrobenzene
• CAS No.: 860585-81-5
• Molecular Formula: C₇H₆INO₃
• Molecular Weight: 279.034
• Hs Code.: 2909309090
• Mol file: 860585-81-5.mol

Synonyms:2-methoxy-4-iodonitrobenzene

Chemical Property of 4-Iodo-2-Methoxy-1-nitrobenzene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

4-Iodo-2-methoxy-1-nitrobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Iodo-2-Methoxy-1-nitrobenzene

There total 2 articles about 4-Iodo-2-Methoxy-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Iodophenol (626-02-8) → 2-methoxy-4-iodonitrobenzene (860585-81-5)

Guidance literature:

Multi-step reaction with 2 steps

1: alcohol; diluted sulfuric acid; sodium nitrate / 15 °C

2: natrium carbonate

With sodium nitrate; ethanol; sulfuric acid; sodium carbonate;

Reference yield:

5-iodo-2-nitrophenol (27783-55-7) + dimethyl sulfate (77-78-1) → 2-methoxy-4-iodonitrobenzene (860585-81-5)

Guidance literature:

With sodium carbonate;

Reference yield: 77.0%

2-methoxy-4-iodonitrobenzene (860585-81-5) → 4-iodo-2-methoxy aniline (338454-80-1)

Guidance literature:

With tin(ll) chloride; In ethanol; for 4h; Reflux;

DOI:10.1021/jm200454y

upstream raw materials:

5-iodo-2-nitrophenol

dimethyl sulfate

3-Iodophenol

Downstream raw materials:

bis-(3-methoxy-4-nitro-phenyl)-disulfide

2-(3-amino-4-methoxyphenyl)-6-methoxy-3-(3,4,5-trimethoxybenzoyl)benzo[b]furan

2-methoxy-4-iodo-N,N-dibenzylaniline

3-N,N-dibenzylamino-4-methoxyphenyltrimethylsilylacetylene