2K⁽¹⁺⁾{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

Base Information

Chemical Name:2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O
CAS No.:89828-34-2
Molecular Formula:2C₄H₈O*C₃₂H₂₀Mo₂O₈P₂*2K
Molecular Weight:1008.74
Hs Code.:

2K<sup>(1+)</sup>*{Mo<sub>2</sub>(CO)8(P(C<sub>6</sub>H<sub>5</sub>)2)2}<sup>(2-)</sup>*2C<sub>4</sub>H<sub>8</sub>O=K<sub>2</sub>{Mo<sub>2</sub>(CO)8(P(C<sub>6</sub>H<sub>5</sub>)2)2}*2C<sub>4</sub>H<sub>8</sub>O

Synonyms:2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

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Chemical Property of 2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

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Technology Process of 2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

There total 2 articles about 2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: bis-μ-diphenylphosphido-octacarbonyldimolybdenum (Mo-Mo)

: potassium tri-sec-butyl-borohydride

: 89828-34-2
2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; Mo-complex was treated with 2 equiv of KB(sec-Bu)3H in THF at 25°C under N2; resulting ppt. was collected; amt. of THF was detd. by (1)H NMR;

Reference yield: 82.0%

: bis-μ-diphenylphosphido-octacarbonyldimolybdenum (Mo-Mo)

: 89828-34-2
2K⁽¹⁺⁾*{Mo₂(CO)8(P(C₆H₅)2)2}^(2-)*2C₄H₈O=K₂{Mo₂(CO)8(P(C₆H₅)2)2}*2C₄H₈O

Guidance literature:: With KB(sec-Bu)3H; In tetrahydrofuran; addn. of 2 equiv KB(sec-C4H9)3H (2.60 mmol) to a suspension of Mo2(CO)8(μ-P(C6H5)2)2 (2.54 mmol) in THF; stirring for ca. 2 h;; filtration; drying; elem. anal.;;
DOI:10.1021/ja00246a018