C₂₃H₂₃⁽²⁾H₂NO₃

Base Information

Chemical Name:C₂₃H₂₃⁽²⁾H₂NO₃
CAS No.:1562377-41-6
Molecular Formula:C₂₃H₂₅NO₃
Molecular Weight:365.441
Hs Code.:

C<sub>23</sub>H<sub>23</sub><sup>(2)</sup>H<sub>2</sub>NO<sub>3</sub>

Synonyms:C₂₃H₂₃⁽²⁾H₂NO₃

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Chemical Property of C₂₃H₂₃⁽²⁾H₂NO₃

Chemical Property:

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Technology Process of C₂₃H₂₃⁽²⁾H₂NO₃

There total 3 articles about C₂₃H₂₃⁽²⁾H₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 889-31-6
5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one

: 1562377-41-6
C₂₃H₂₃⁽²⁾H₂NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Molecular sieve; Inert atmosphere

1.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 5 h / 0 °C / Molecular sieve; Inert atmosphere

2.2: 2 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

3.1: tetradeuterioacetic acid / Inert atmosphere

With n-butyllithium; tetradeuterioacetic acid; potassium hexamethylsilazane; In tetrahydrofuran;
DOI:10.1021/ol4034447

Reference yield:

: 1562377-09-6
C₂₃H₂₅NO₃

: 1562377-41-6
C₂₃H₂₃⁽²⁾H₂NO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 5 h / 0 °C / Molecular sieve; Inert atmosphere

1.2: 2 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

2.1: tetradeuterioacetic acid / Inert atmosphere

With tetradeuterioacetic acid; potassium hexamethylsilazane; In tetrahydrofuran;
DOI:10.1021/ol4034447

Reference yield:

: 100-46-9
benzylamine

: 1562377-41-6
C₂₃H₂₃⁽²⁾H₂NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid; sodium sulfate / benzene / 85 °C / Sealed tube; Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Molecular sieve; Inert atmosphere

2.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran / 5 h / 0 °C / Molecular sieve; Inert atmosphere

3.2: 2 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

4.1: tetradeuterioacetic acid / Inert atmosphere

With n-butyllithium; tetradeuterioacetic acid; potassium hexamethylsilazane; toluene-4-sulfonic acid; sodium sulfate; In tetrahydrofuran; benzene;
DOI:10.1021/ol4034447