C₂₃H₃₁BrO₃

Base Information

Chemical Name:C₂₃H₃₁BrO₃
CAS No.:1213270-15-5
Molecular Formula:C₂₃H₃₁BrO₃
Molecular Weight:435.401
Hs Code.:

C<sub>23</sub>H<sub>31</sub>BrO<sub>3</sub>

Synonyms:C₂₃H₃₁BrO₃

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Chemical Property of C₂₃H₃₁BrO₃

Chemical Property:

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Technology Process of C₂₃H₃₁BrO₃

There total 4 articles about C₂₃H₃₁BrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1213270-08-6
C₂₁H₂₉BrO₂

: 108-24-7
acetic anhydride

: 1213270-15-5
C₂₃H₃₁BrO₃

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1021/ol100214X

Reference yield:

: 106-41-2
4-bromo-phenol

: 1213270-15-5
C₂₃H₃₁BrO₃

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl hydrogen phosphate / dichloromethane / 4.5 h / 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 1.17 h / 0 °C / Inert atmosphere

With dmap; diphenyl hydrogen phosphate; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2011.06.054

Reference yield:

: 87-44-5
β-caryophyllene

: 1213270-15-5
C₂₃H₃₁BrO₃

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.75 h / 0 °C / Inert atmosphere

2: diphenyl hydrogen phosphate / dichloromethane / 4.5 h / 0 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 1.17 h / Inert atmosphere

With dmap; diphenyl hydrogen phosphate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1039/c1ob06363d