[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

Base Information

Chemical Name:[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]
CAS No.:925941-62-4
Molecular Formula:C₂₈H₃₀NO₅PPdS
Molecular Weight:630.01
Hs Code.:

Synonyms:[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

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Chemical Property of [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

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Technology Process of [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

There total 4 articles about [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 108-48-5
2,6-dimethylpyridine

: 875765-21-2
CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)^(1-)*HN(CH(CH₃)2)2C₂H₅⁽¹⁺⁾=HN(CH(CH₃)2)2C₂H₅CH₃PdCl(O₃SC₆H₄P(C₆H₄OCH₃)2)

: 925941-62-4
[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

Guidance literature:: With potassium carbonate; In dichloromethane; treatment of Pd complex with 2,6-lutidine and K2CO3 for 1 h at room temp. in CH2Cl2;
DOI:10.1021/ja0725504

Reference yield:

: 108-48-5
2,6-dimethylpyridine

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 257290-43-0
2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid

: 925941-62-4
[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(2,6-lutidine)]

Guidance literature:: In dichloromethane; byproducts: (CH3)2C5H3NHCl; treatment of phospine ligand with 2,6-lutidine for 10 min at room temp. in CH2Cl2, treatment with PdMeCl(C8H12) for 5 h at room temp.;
DOI:10.1021/ja0725504