o-n-hex-1-ynylbenzyl bromide

Base Information

Chemical Name:o-n-hex-1-ynylbenzyl bromide
CAS No.:442904-00-9
Molecular Formula:C₁₃H₁₅Br
Molecular Weight:251.166
Hs Code.:

Synonyms:o-n-hex-1-ynylbenzyl bromide

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Chemical Property of o-n-hex-1-ynylbenzyl bromide

Chemical Property:

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Technology Process of o-n-hex-1-ynylbenzyl bromide

There total 3 articles about o-n-hex-1-ynylbenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 210964-21-9
[2-(hex-1-yn-1-yl)phenyl]methanol

: 442904-00-9
o-n-hex-1-ynylbenzyl bromide

Guidance literature:: With pyridine; phosphorus tribromide; In chloroform; at 20 ℃;
DOI:10.1039/b111045b

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 442904-00-9
o-n-hex-1-ynylbenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CuI / PdCl₂(PPh₃)2 / benzene / 20 °C

2: 78 percent / PBr₃; pyridine / CHCl₃ / 20 °C

With pyridine; copper(l) iodide; phosphorus tribromide; bis-triphenylphosphine-palladium(II) chloride; In chloroform; benzene;
DOI:10.1039/b111045b

Reference yield:

: 693-02-7
hex-1-yne

: 442904-00-9
o-n-hex-1-ynylbenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CuI / PdCl₂(PPh₃)2 / benzene / 20 °C

2: 78 percent / PBr₃; pyridine / CHCl₃ / 20 °C

With pyridine; copper(l) iodide; phosphorus tribromide; bis-triphenylphosphine-palladium(II) chloride; In chloroform; benzene;
DOI:10.1039/b111045b