(2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Base Information

Chemical Name:(2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester
CAS No.:77733-82-5
Molecular Formula:C₂₂H₂₁NO₄
Molecular Weight:363.413
Hs Code.:

Synonyms:(2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Suppliers and Price of (2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Chemical Property:

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Technology Process of (2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

There total 6 articles about (2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 77733-82-5
(2E)-6-<2-(3-Cyan-trans-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

: 77733-86-9
(2α,3β,3aβ,11bα)-2-Cyan-2,3,3a,5,6,11b-hexahydro-2-phenyl-4H-furo<3,2-e><1>benzoxocin-3-carbonsaeure-methylester

: 77733-82-5
(2E)-6-<2-(3-Cyan-cis-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Guidance literature:: In 2,2,4-trimethylpentane; at 215 ℃; for 7h; Yields of byproduct given;

Reference yield:

: 40359-46-4
4-(2-formylphenoxy)-butyric acid ethyl ester

: 77733-82-5
(2E)-6-<2-(3-Cyan-cis-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / p-TsOH / benzene / Heating

2: 92 percent / LiAlH₄ / diethyl ether / 1 h / Heating

3: 76 percent / pyridinium dichromate / CH₂Cl₂ / 36 h

4: 1.) KOtBu, 2.) aq. HCl / 1.) DMF, 3h, 2.) ether, CH₂Cl₂, 6 h

5: 1M KOtBu / 2-methyl-propan-2-ol; benzene / 72 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; dipyridinium dichromate; potassium tert-butylate; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; tert-butyl alcohol; benzene;

Reference yield:

: 90-02-8
salicylaldehyde

: 77733-82-5
(2E)-6-<2-(3-Cyan-cis-3-phenyl-2-oxiranyl)phenoxy>-2-hexensaeure-methylester

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 95 percent / p-TsOH / benzene / Heating

3: 92 percent / LiAlH₄ / diethyl ether / 1 h / Heating

4: 76 percent / pyridinium dichromate / CH₂Cl₂ / 36 h

5: 1.) KOtBu, 2.) aq. HCl / 1.) DMF, 3h, 2.) ether, CH₂Cl₂, 6 h

6: 1M KOtBu / 2-methyl-propan-2-ol; benzene / 72 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; dipyridinium dichromate; potassium tert-butylate; potassium carbonate; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;