C₇₄H₁₄₄O₁₁Si₆

Base Information

Chemical Name:C₇₄H₁₄₄O₁₁Si₆
CAS No.:902132-46-1
Molecular Formula:C₇₄H₁₄₄O₁₁Si₆
Molecular Weight:1378.46
Hs Code.:

C<sub>74</sub>H<sub>144</sub>O<sub>11</sub>Si<sub>6</sub>

Synonyms:C₇₄H₁₄₄O₁₁Si₆

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Chemical Property of C₇₄H₁₄₄O₁₁Si₆

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Technology Process of C₇₄H₁₄₄O₁₁Si₆

There total 31 articles about C₇₄H₁₄₄O₁₁Si₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 902132-44-9
C₄₄H₇₄O₁₁Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 902132-46-1
C₇₄H₁₄₄O₁₁Si₆

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 1.5h;
DOI:10.1039/b602020h

Reference yield:

: 902132-11-0
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexenal

: 902132-46-1
C₇₄H₁₄₄O₁₁Si₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 - 0 °C

2.1: 93 percent / imidazole; 4-DMAP / CH₂Cl₂ / 2 h / 20 °C

3.1: O₃ / CH₂Cl₂ / -78 °C

3.2: 98 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

4.1: 98 percent / benzene / 16 h / 70 °C

5.1: 99 percent / DIBAL-H / tetrahydrofuran / 0.5 h / 0 °C

6.1: Et₃N / tetrahydrofuran / 1 h / 0 °C

7.1: 2.004 g / LiBr / tetrahydrofuran / 0.75 h / 25 °C

8.1: LDA / tetrahydrofuran / 1.5 h / -78 °C

8.2: 84 percent / tetrahydrofuran / 1 h / -78 °C

9.1: LDA / tetrahydrofuran / 2 h / -78 °C

9.2: tetrahydrofuran / 4 h / -78 °C

10.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

11.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

12.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; n-butyllithium; oxalic acid; diisobutylaluminium hydride; toluene-4-sulfonic acid; ozone; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; benzene; 4.1: Wittig reaction;
DOI:10.1039/b602020h

Reference yield:

: 902131-93-5
C₃₉H₇₇IO₅Si₃

: 902132-46-1
C₇₄H₁₄₄O₁₁Si₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 90 percent / DDQ; aq. pH 7.0 buffer / CH₂Cl₂ / 1 h / 25 °C

2.1: 65 percent / pyridine; 4-DMAP / CH₂Cl₂ / 22 h / 0 - 25 °C

3.1: LDA / tetrahydrofuran / 2 h / -78 °C

3.2: tetrahydrofuran / 4 h / -78 °C

4.1: 1.811 g / aq. (CO₂H)2 / diethyl ether / 40 h / 25 °C

5.1: 64 percent / TsOH*H₂O / methanol; CH₂Cl₂ / 20 h / 25 °C

6.1: 54 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h / 0 °C

With pyridine; 2,6-dimethylpyridine; dmap; oxalic acid; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/b602020h