(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

Base Information

Chemical Name:(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester
CAS No.:261347-59-5
Molecular Formula:C₂₆H₂₈NO₆P
Molecular Weight:481.485
Hs Code.:

Synonyms:(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

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Chemical Property of (S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

There total 1 articles about (S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2440-79-1
N-acetyl-L-tyrosine methyl ester

: 67746-43-4
dibenzyl N,N-diethylphosphoramidite

: 261347-59-5
(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

Guidance literature:: With 1H-tetrazole; In tetrahydrofuran; at 25 ℃; for 1h;
DOI:10.1021/jo991616d

Reference yield:

: 261347-59-5
(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

: 244210-96-6
N-acetyl-L-tyrosine dibenzyl phosphate methyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/jo991616d

Reference yield:

: 261347-59-5
(S)-2-Acetylamino-3-[4-(bis-benzyloxy-phosphanyloxy)-phenyl]-propionic acid methyl ester

: 261347-60-8
N-acetyl-L-tyrosinephosphate methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

2: 91 percent / H₂ / 5percent Pd/C / methanol / 3 h / 25 °C

With hydrogen; 3-chloro-benzenecarboperoxoic acid; 5percent Pd/C; In methanol; dichloromethane; 1: Oxidation / 2: debenzylation;
DOI:10.1021/jo991616d