H-DL-delta-Hydroxy-DL-Lys(Boc)-OH

Base Information

• Chemical Name: H-DL-delta-Hydroxy-DL-Lys(Boc)-OH
• CAS No.: 305820-28-4
• Molecular Formula: C₁₁H₂₂N₂O₅
• Molecular Weight: 262.306
• DSSTox Substance ID: DTXSID50449460
• Mol file: 305820-28-4.mol

Synonyms:H-DL-delta-Hydroxy-DL-Lys(Boc)-OH;305820-28-4;H-DL-Hyl(Boc)-OH;2-amino-5-hydroxy-6-[(2-methylpropan-2-yl)oxycarbonylamino]hexanoic Acid;H-DL-d-Hydroxy-DL-Lys(Boc)-OH;SCHEMBL12463713;DTXSID50449460;H-DL--Hydroxy-DL-Lys(Boc)-OH;H-DL-gamma-Hydroxy-DL-Lys(Boc)-OH;2-AMINO-6-[(TERT-BUTOXYCARBONYL)AMINO]-5-HYDROXYHEXANOIC ACID

Chemical Property of H-DL-delta-Hydroxy-DL-Lys(Boc)-OH

Chemical Property:

• Boiling Point: 464.4±45.0 °C(Predicted)
• PKA: 2.50±0.28(Predicted)
• PSA: 125.37000
• Density: 1 +-.0.06 g/cm3(Predicted)
• LogP: 0.96880
• Storage Temp.: -15°C
• XLogP3: -2.6
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 8
• Exact Mass: 262.15287181
• Heavy Atom Count: 18
• Complexity: 288

Purity/Quality:

97% ^*data from raw suppliers

H-DL-D-HYDROXY-DL-LYS(BOC)-OH 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)OC(=O)NCC(CCC(C(=O)O)N)O
• Uses: N6-[(1,1-Dimethylethoxy)carbonyl]-5-hydroxy-lysine is used in the synthesis and characterization of a collagen model δ-?O-?phosphohydroxylysine-?containing peptide.

Technology Process of H-DL-delta-Hydroxy-DL-Lys(Boc)-OH

There total 1 articles about H-DL-delta-Hydroxy-DL-Lys(Boc)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

di-tert-butyl dicarbonate (24424-99-5) + δ-hydroxylysine hydrochloride (2219-28-5) → 2-amino-6-(tert-butoxycarbonylamino)-5-hydroxyhexanoic acid (305820-28-4)

Guidance literature:

δ-hydroxylysine hydrochloride; With copper(ll) sulfate pentahydrate; sodium hydrogencarbonate; at 20 ℃; for 0.166667h;

di-tert-butyl dicarbonate; In acetone; at 20 ℃; for 18h;

With 8-quinolinol; In water; at 20 ℃; for 18h;

DOI:10.1021/ja202799r

upstream raw materials:

di-tert-butyl dicarbonate

δ-hydroxylysine hydrochloride