Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2

Base Information

• Chemical Name: Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2
• CAS No.: 913356-00-0
• Molecular Formula: C₃₄H₃₆Cl₂N₄O₈Re₂
• Molecular Weight: 1072
• Mol file: 913356-00-0.mol

Synonyms:Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2

Chemical Property of Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2

Chemical Property:

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Technology Process of Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2

There total 1 articles about Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₂(OAc)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

cis-diacetatotetrachloro(H2O)2dirhenate(III) + N,N'-di-(3-methoxy)phenylformamidine → Re2(N,N'-di(3-methoxyphenyl)formamidine(1-))2Cl2(OAc)2 (913356-00-0)

Guidance literature:

With N(CH₂CH₃)3; In tetrahydrofuran; (under Ar); Re-complex, ligand and N(CH2CH3)3 mixed in THF, refluxed for24 h; filtered, solvent removed, ppt. dissolved in CH2Cl2, filtered, solvent removed, dissolved in MeOH and ethyl acetate, ethyl acetate soln. reduced, layered with hexane, slow evapn. of ethyl acetate soln.; elem. anal.;

DOI:10.1016/j.ica.2006.06.044