2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate

Base Information

• Chemical Name: 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate
• CAS No.: 154145-31-0
• Molecular Formula: C₄₂H₃₀O₄P₂
• Molecular Weight: 660.645
• Mol file: 154145-31-0.mol

Synonyms:2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate

Chemical Property of 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate

There total 5 articles about 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,4,6-tris(triphenylphosphoranylidene)cyclohexane-1,3,5-trione → 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate (154145-31-0)

Guidance literature:

With 2-[(4-methylphenyl)sulfonyl]-3-phenyl-oxaziridine;

Reference yield: 53.0%

2,3,5,6-tetrafluoro-1,4-benzoquinone (527-21-9,777826-79-6) + triphenylphosphine (603-35-0) → 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate (154145-31-0)

Guidance literature:

In 1,4-dioxane; water; for 24h;

DOI:10.1016/j.jfluchem.2015.08.018

Reference yield: 51.0%

4,5-difluoro-3,6-dioxo-2-(triphenylphosphonio)cyclohexa-1,4-dien-1-olate + triphenylphosphine (603-35-0) → 2,5-dioxo-4,6-bis(triphenylphosphonio)cyclohexa-3,6-diene-1,3-diolate (154145-31-0)

Guidance literature:

4,5-difluoro-3,6-dioxo-2-(triphenylphosphonio)cyclohexa-1,4-dien-1-olate; triphenylphosphine; In 1,4-dioxane; for 240h;

With water; In 1,4-dioxane; for 48h;

DOI:10.1016/j.jfluchem.2015.08.018

upstream raw materials:

triphenylphosphine

2,3,5,6-tetrafluoro-1,4-benzoquinone