Technology Process of 2-geranyl-3,5-dimethoxy-3′-prenyl-4′,5′-dihydroxy-(E)-stilbene
There total 6 articles about 2-geranyl-3,5-dimethoxy-3′-prenyl-4′,5′-dihydroxy-(E)-stilbene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
at 20 ℃;
for 42h;
Inert atmosphere;
DOI:10.1021/np4009046
- Guidance literature:
-
Multi-step reaction with 5 steps
1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; copper(l) iodide / hexane; diethyl ether / -10 °C / Inert atmosphere
2: toluene-4-sulfonic acid / methanol / 2.5 h / 20 °C / Inert atmosphere
3: manganese(IV) oxide / dichloromethane / Inert atmosphere
4: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0 °C / Inert atmosphere
5: toluene-4-sulfonic acid / methanol / 42 h / 20 °C / Inert atmosphere
With
manganese(IV) oxide; copper(l) iodide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium hexamethylsilazane; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1021/np4009046
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0 °C / Inert atmosphere
2: toluene-4-sulfonic acid / methanol / 42 h / 20 °C / Inert atmosphere
With
potassium hexamethylsilazane; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; toluene;
DOI:10.1021/np4009046
