pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

Base Information

Chemical Name:pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate
CAS No.:839719-68-5
Molecular Formula:C₂₉H₁₈F₅NO₄
Molecular Weight:539.458
Hs Code.:

Synonyms:pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

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Technology Process of pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

There total 1 articles about pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 14533-84-7
pentafluorophenyl trifloroacetate

: 102410-65-1,163883-97-4
Fmoc-Phg-OH

: 839719-68-5
pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm049906w

Reference yield: 79.0%

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 839719-68-5
pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

: 111524-86-8
methyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-2-phenylacetamido)-3-phenylpropanoate

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide; for 0.0125h; microwave irradiation;

Reference yield:

: 86060-93-7
Fmoc-Tyr(tBu)-OPfp

: 797751-68-9
N^α-Fmoc-L-Asn-OPfp

: 839719-68-5
pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate

: YFDD

Guidance literature:: N^α-Fmoc-L-Asn-OPfp; With pyrazolone orange; C₁₄H₁₂FeO₆^(1-)*Na⁽¹⁺⁾; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Combinatorial reaction / High throughput screening (HTS); Inert atmosphere; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide;

Fmoc-Tyr(tBu)-OPfp; N^α-Fmoc-L-Asn-OPfp; pentafluorophenyl L-α-[(9H-fluoren-9-ylmethoxycarbonyl)amino]-α-benzeneethanoate; Further stages;
DOI:10.1002/anie.200801616