salicylaldehyde-(N-benzyl oxime )

Base Information

• Chemical Name: salicylaldehyde-(N-benzyl oxime )
• CAS No.: 22687-11-2
• Molecular Formula: C₁₄H₁₃NO₂
• Molecular Weight: 227.263
• Mol file: 22687-11-2.mol

Synonyms:salicylaldehyde-(N-benzyl oxime )

Chemical Property of salicylaldehyde-(N-benzyl oxime )

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of salicylaldehyde-(N-benzyl oxime )

There total 2 articles about salicylaldehyde-(N-benzyl oxime ) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-benzylhydroxylamine hydrochloride (29601-98-7) + salicylaldehyde (90-02-8) → salicylaldehyde-(N-benzyl oxime ) (22687-11-2)

Guidance literature:

In glycerol; at 60 - 80 ℃; for 0.5h; Green chemistry;

DOI:10.1007/s12039-019-1677-7

Reference yield:

→ salicylaldehyde-(N-benzyl oxime ) (22687-11-2)

Guidance literature:

entspr. Aldehyd, N-Benzyl-hydroxylamin;

Reference yield: 97.0%

salicylaldehyde-(N-benzyl oxime ) (22687-11-2) + catechol butyl borate (3488-87-7) → 8-CH2Ph-6,6-(1,2-phenylenedioxy)-5,7-dioxa-8-aza-6-bora-6,7-dihydro-5H-benzocycloheptene + butan-1-ol (71-36-3)

Guidance literature:

In benzene; to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. recrystd. from THF/petroleum ether, elem. anal.;

DOI:10.1016/S0022-328X(00)98570-X

upstream raw materials:

N-benzylhydroxylamine hydrochloride

salicylaldehyde

Downstream raw materials:

2-acetoxy-benzoic acid benzylamide

N,O-dibenzoyl-N-benzylhydroxylamine

salicylaldehyde

N-benzyl hydroxylalmine