3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

Base Information

Chemical Name:3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide
CAS No.:146072-99-3
Molecular Formula:C₂₄H₃₄N₂O₆S
Molecular Weight:478.61
Hs Code.:

Synonyms:3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

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Chemical Property of 3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

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Technology Process of 3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

There total 7 articles about 3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: C₈H₁₆LiNO

: 144024-38-4
3-(1,3-dioxolan-2-yl)-1-<1-(phenylsulfonyl)-3-pyrrolyl>-1-propanone

: 146072-99-3
3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

Guidance literature:: In tetrahydrofuran; at -85 - -70 ℃; for 0.5h;
DOI:10.1248/cpb.40.2338

Reference yield:

: 81453-98-7
3-acetyl-1-(phenylsulfonyl)pyrrole

: 146072-99-3
3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

Guidance literature:: Multi-step reaction with 6 steps

1: SeO₂ / dioxane; H₂O / 4 h / Heating

2: NaBH₄ / ethanol / 1 h / Ambient temperature

3: aq. NaIO₄ / diethyl ether / 0.67 h / Ambient temperature

4: 98 percent / tetrahydrofuran / 0.17 h / -20 °C

5: 82 percent / MnO₂ / benzene / 1 h / Heating

6: 96 percent / tetrahydrofuran / 0.5 h / -85 - -70 °C

With manganese(IV) oxide; sodium tetrahydroborate; sodium periodate; selenium(IV) oxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water; benzene;
DOI:10.1248/cpb.40.2338

Reference yield:

: 88075-95-0
1-(phenylsulfonyl)-1H-pyrrole-3-carbaldehyde

: 146072-99-3
3-(1-Benzenesulfonyl-1H-pyrrol-3-yl)-5-[1,3]dioxolan-2-yl-3-hydroxy-pentanoic acid dipropylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / tetrahydrofuran / 0.17 h / -20 °C

2: 82 percent / MnO₂ / benzene / 1 h / Heating

3: 96 percent / tetrahydrofuran / 0.5 h / -85 - -70 °C

With manganese(IV) oxide; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.40.2338